Tensile-WAXD Apparatus: An Improved and Accurate System for the<italic style="font-style: italic">In situ</italic> Study of Extension-induced Segmental Orientation in Highly Stretched Elastomer

Xiang Shi

doi:10.1007/s10118-024-3201-x

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Tensile-WAXD Apparatus: An Improved and Accurate System for theIn situ Study of Extension-induced Segmental Orientation in Highly Stretched Elastomer

RESEARCH ARTICLE | Updated：2024-12-03

- Tensile-WAXD Apparatus: An Improved and Accurate System for theIn situ Study of Extension-induced Segmental Orientation in Highly Stretched Elastomer
- Tensile-WAXD Apparatus: An Improved and Accurate System for theIn situ Study of Extension-induced Segmental Orientation in Highly Stretched Elastomer
- 高分子科学（英文版） 2024年42卷第12期页码：2002-2010
- Affiliations：
  
  a.Center for Advanced Material Diagnostic Technology, Shenzhen Technology University, Shenzhen 518118, China
  b.Laboratoire de Physique des Solides, CNRS, Université Paris-Sud, Université Paris-Saclay, Orsay 91400, France
- Author bio：
  
  shixiang@sztu.edu.cn
- Funds：
  
  The authors gratefully appreciate the technical support and assistance from the staff of the scientific teams “MATTER AND RADIATION” in Laboratoire de Physique des Solides, Université Paris-Saclay, and the financial support of China CSC Scholarship (No. 201604910522).;Electronic supplementary information (ESI) is available free of charge in the online version of this article at http://doi.org/10.1007/s10118-024-3201-x.
- DOI：10.1007/s10118-024-3201-x
  中图分类号：
- 收稿：2024-05-26，
  
  修回：2024-06-11，
  
  录用：2024-07-04，
  
  网络首发：2024-10-10，
  
  纸质出版：2024-12-01
- Accepted：
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Shi, X. Tensile-WAXD apparatus: an improved and accurate system for the in situ study of extension-induced segmental orientation in highly stretched elastomer. Chinese J. Polym. Sci. 2024, 42, 2002–2010

Xiang Shi. Tensile-WAXD Apparatus: An Improved and Accurate System for theIn situ Study of Extension-induced Segmental Orientation in Highly Stretched Elastomer[J]. Chinese Journal of Polymer Science, 2024, 42(12): 2002-2010. DOI: 10.1007/s10118-024-3201-x.
Shi, X. Tensile-WAXD apparatus: an improved and accurate system for the in situ study of extension-induced segmental orientation in highly stretched elastomer. Chinese J. Polym. Sci. 2024, 42, 2002–2010 DOI： 10.1007/s10118-024-3201-x.

Xiang Shi. Tensile-WAXD Apparatus: An Improved and Accurate System for theIn situ Study of Extension-induced Segmental Orientation in Highly Stretched Elastomer[J]. Chinese Journal of Polymer Science, 2024, 42(12): 2002-2010. DOI: 10.1007/s10118-024-3201-x. DOI：

摘要

By utilizing mortise-like clamping jaws and dogbone-shaped specimens

an improved X-ray apparatus that combines tensile testing and X-ray diffraction has been designed and constructed to investigate the “stress-deformation-segmental orientation” relationship in elastomers with high extensibilities. Due to the minimization of experimental errors from sample slippage or premature fracture

this setup allows for the simultaneous recording of high-quality mechanical responses and 2D diffraction patterns. Furthermore

the local extension ratio can be accurately determined based on thickness variation

and the Hermans' orientation function was demonstrated to be a reliable method with high accuracy to calculate the segmental orientation parameter ⟨

⟩ in elastomeric samples under high degree of stretching.

Abstract

An improved X-ray apparatus that combines tensile testing and X-ray diffraction has been designed and constructed to conduct time-resolved experiments during uniaxial stretching. By utilizing mortise-like clamping jaws and dogbone-shaped specimens

this setup allows for the simultaneous recording of high-quality mechanical responses and 2D diffraction patterns due to the minimization of experimental errors from sample slippage or premature fracture. Furthermore

the local extension ratio can be accurately determined based on thickness variation

and the Hermans' orientation function was demonstrated to be a reliable method with high accuracy to calculate the segmental orientation parameter

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in elastomeric samples under high degree of stretching. In summary

this innovative tensile-WAXD instrument has proven to be a promising and powerful technique for investigating the “stress-deformation-segmental orientation” relationship in elastomers with high extensibilities.

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references

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Tensile-WAXD Apparatus: An Improved and Accurate System for theIn situ Study of Extension-induced Segmental Orientation in Highly Stretched Elastomer

Tensile-WAXD Apparatus: An Improved and Accurate System for theIn situ Study of Extension-induced Segmental Orientation in Highly Stretched Elastomer

DOI：10.1007/s10118-024-3201-x

摘要

Abstract

关键词

Keywords

references