Mixed Matrix Membranes of Polysulfone/Polyimide Reinforced with Modified Zeolite Based Filler: Preparation, Properties and Application

Sedra Tul Muntha; Muhammad Siddiq; Ayesha Kausar; Anum Khan

doi:10.1007/s10118-018-2021-2

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Mixed Matrix Membranes of Polysulfone/Polyimide Reinforced with Modified Zeolite Based Filler: Preparation, Properties and Application

PAPERS | Updated：2021-02-18

- Mixed Matrix Membranes of Polysulfone/Polyimide Reinforced with Modified Zeolite Based Filler: Preparation, Properties and Application
- Mixed Matrix Membranes of Polysulfone/Polyimide Reinforced with Modified Zeolite Based Filler: Preparation, Properties and Application
- Chinese Journal of Polymer Science 2018年36卷第1期页码：65-77
- Affiliations：
  
  a.Department of Chemistry, Quaid i Azam University, Islamabad 45320, Pakistan
  b.Department of Microbiology, Quaid i Azam University, Islamabad 45320, Pakistan
- Author bio：
  
  Muhammad Siddiq, E-mail m_sidiq12@yahoo.com
- Funds：
- DOI：10.1007/s10118-018-2021-2
  中图分类号：
- 收稿：2017-07-21，
  
  录用：2017-8-17，
  
  网络首发：2017-10-30，
  
  纸质出版：2018-01-05
- Accepted：
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Sedra Tul Muntha, Muhammad Siddiq, Ayesha Kausar, 等. Mixed Matrix Membranes of Polysulfone/Polyimide Reinforced with Modified Zeolite Based Filler: Preparation, Properties and Application[J]. Chinese Journal of Polymer Science, 2018,36(1):65-77.

Sedra Tul Muntha, Muhammad Siddiq, Ayesha Kausar, et al. Mixed Matrix Membranes of Polysulfone/Polyimide Reinforced with Modified Zeolite Based Filler: Preparation, Properties and Application[J]. Chinese Journal of Polymer Science, 2018, 36(1): 65-77.
Sedra Tul Muntha, Muhammad Siddiq, Ayesha Kausar, 等. Mixed Matrix Membranes of Polysulfone/Polyimide Reinforced with Modified Zeolite Based Filler: Preparation, Properties and Application[J]. Chinese Journal of Polymer Science, 2018,36(1):65-77. DOI： 10.1007/s10118-018-2021-2.

Sedra Tul Muntha, Muhammad Siddiq, Ayesha Kausar, et al. Mixed Matrix Membranes of Polysulfone/Polyimide Reinforced with Modified Zeolite Based Filler: Preparation, Properties and Application[J]. Chinese Journal of Polymer Science, 2018, 36(1): 65-77. DOI： 10.1007/s10118-018-2021-2.

摘要

Abstract

In this work

polysulfone/polyimide (PSf/PI) mixed matrix membranes were fabricated by reinforcement of modified zeolite (MZ) particles through solution casting method for investigation of antibacterial activity against two gram negative bacteria (

Salmonella typhi

Klebsella pneumonia

) and two gram positive bacteria (

Staphylococcus aureus

Bacillus subtilis

). The modified zeolite particles were incorporated to PSf and PI matrix and the influence of these particles on thermal

mechanical and structural properties was evaluated. The morphological evolution was investigated through scanning electron microscopy (SEM) and transmission electron microscopy (TEM) analysis

which revealed good compatibility between organic polymer matrix and inorganic filler. Mechanical stability was investigated by tensile testing while thermal analysis was evaluated by thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC). This revealed improvement in thermal properties with increasing filler concentration from 1 wt% to 10 wt%. Structural analysis was successfully done using X-ray diffraction analysis (XRD) and Fourier transform infrared (FTIR) spectroscopy. Solvent content of fabricated mixed matrix membranes was observed to decrease while moving from more hydrophilic to less hydrophilic solvent. However

addition of filler content enhanced the porosity of fabricated membranes. The synthesized mixed matrix membranes exhibited good antibacterial activity and the highest activity was shown by PSf/PI/MZ mixed matrix membrane. Therefore

the combination effect of PSf

PI and MZ sufficiently enhanced the antibacterial activity of mixed matrix membranes.

关键词

Keywords

references

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