The Effect of Self-nucleation on Isothermal Crystallization Kinetics of Poly (butylene succinate)(PBS) Investigated by Differential Fast Scanning Calorimetry

Jing Jiang; Evgeny Zhuravlev; Wen-bing Hu; Christoph Schickc; Dong-shan Zhou

doi:10.1007/s10118-017-1942-5

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The Effect of Self-nucleation on Isothermal Crystallization Kinetics of Poly (butylene succinate)(PBS) Investigated by Differential Fast Scanning Calorimetry

Papers | Updated：2021-02-18

- The Effect of Self-nucleation on Isothermal Crystallization Kinetics of Poly (butylene succinate)(PBS) Investigated by Differential Fast Scanning Calorimetry
- The Effect of Self-nucleation on Isothermal Crystallization Kinetics of Poly (butylene succinate)(PBS) Investigated by Differential Fast Scanning Calorimetry
- Chinese Journal of Polymer Science 2017年35卷第8期页码：1009-1019
- Affiliations：
  
  a.Department of Polymer Science and Engineering, School of Chemistry and Chemical Engineering, State Key Laboratory of Coordination Chemistry, Nanjing University, Nanjing 210023, China
  b.School of Physical Science and Technology, Xinjiang Key Laboratory and Phase Transitions and Microstructures in Condensed Matters, Yili Normal University, Yining 835000, China
  c.University of Rostock, Institute of Physics, Wismarsche Strasse 43-45, 18051 Rostock, Germany
- Author bio：
  
  Dong-shan Zhou (周东山), E-mail: dzhou@nju.edu.cn
- Funds：
  
  the National Natural Science Foundation of China(21474049);the National Natural Science Foundation of China(51673094);the National Natural Science Foundation of China(21404055);the Shenzhen Science and Technology Innovation Committee(JCYJ20160531151102203);the Shenzhen Science and Technology Innovation Committee(JCYJ20160608140827794);Tianshan Scholars Program by Yili Normal University
- DOI：10.1007/s10118-017-1942-5
  中图分类号：
- 收稿：2016-12-30，
  
  修回：2017-1-23，
  
  录用：2017-2-8，
  
  纸质出版：2017-08
- Accepted：
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Jing Jiang, Evgeny Zhuravlev, Wen-bing Hu, 等. The Effect of Self-nucleation on Isothermal Crystallization Kinetics of Poly (butylene succinate)(PBS) Investigated by Differential Fast Scanning Calorimetry[J]. Chinese Journal of Polymer Science, 2017,35(8):1009-1019.

Jing Jiang, Evgeny Zhuravlev, Wen-bing Hu, et al. The Effect of Self-nucleation on Isothermal Crystallization Kinetics of Poly (butylene succinate)(PBS) Investigated by Differential Fast Scanning Calorimetry[J]. Chinese Journal of Polymer Science, 2017, 35(8): 1009-1019.
Jing Jiang, Evgeny Zhuravlev, Wen-bing Hu, 等. The Effect of Self-nucleation on Isothermal Crystallization Kinetics of Poly (butylene succinate)(PBS) Investigated by Differential Fast Scanning Calorimetry[J]. Chinese Journal of Polymer Science, 2017,35(8):1009-1019. DOI： 10.1007/s10118-017-1942-5.

Jing Jiang, Evgeny Zhuravlev, Wen-bing Hu, et al. The Effect of Self-nucleation on Isothermal Crystallization Kinetics of Poly (butylene succinate)(PBS) Investigated by Differential Fast Scanning Calorimetry[J]. Chinese Journal of Polymer Science, 2017, 35(8): 1009-1019. DOI： 10.1007/s10118-017-1942-5.

摘要

Abstract

Differential fast scanning calorimetry (DFSC) was employed on the study of self-nucleation behavior of poly(butylene succinate) (PBS). The ultra-fast cooling ability of DFSC allows investigating the effect of self-nucleation on the isothermal crystallization kinetics over a wide temperature range. Crystallization half-time

instead of crystallization peak temperature

was used to describe the self-nucleation behavior

and the self-nucleation domain for the samples crystallized at different temperatures was determined. Due to the competition between homogenous nucleation and self-nuclei

the effect of self-nucleation was less pronounced at high supercooling than that for the sample isothermally crystallized at higher temperature. An efficiency scale to judge the efficiency of nucleating agents from the crystallization half-time was also introduced in this work.

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references

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