Effects of Ultra-high Temperature Treatment on the Microstructure of Carbon Fibers

Wei-wei Li; Kang Hong-liangKang; Jian Xu; Rui-gang Liu

doi:10.1007/s10118-017-1922-9

Your Location：

Home >

Browse articles >

Effects of Ultra-high Temperature Treatment on the Microstructure of Carbon Fibers

Papers | Updated：2021-02-18

- Effects of Ultra-high Temperature Treatment on the Microstructure of Carbon Fibers
- Effects of Ultra-high Temperature Treatment on the Microstructure of Carbon Fibers
- Chinese Journal of Polymer Science 2017年35卷第6期页码：764-772
- Affiliations：
  
  a.Laboratory of Polymer Physics and Chemistry, Beijing National Laboratory for Molecular Science, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China
  b.University of Chinese Academy of Sciences, Beijing 100049, China
- Author bio：
  
  Jian Xu (徐坚), E-mail: jxu@iccas.ac.cn
  Rui-gang Liu (刘瑞刚), E-mail: rgliu@iccas.ac.cn
- Funds：
  
  This work was financially supported by the National High Technology Research and Development Program of China(863 Program, No. 2015AA03A204)
- DOI：10.1007/s10118-017-1922-9
  中图分类号：
- 收稿：2016-09-18，
  
  修回：2016-11-30，
  
  录用：2016-12-2，
  
  纸质出版：2017-06-05
- Accepted：
Scan QR Code
Wei-wei Li, Kang Hong-liangKang, Jian Xu, 等. Effects of Ultra-high Temperature Treatment on the Microstructure of Carbon Fibers[J]. Chinese Journal of Polymer Science, 2017,35(6):764-772.

Wei-wei Li, Kang Hong-liangKang, Jian Xu, et al. Effects of Ultra-high Temperature Treatment on the Microstructure of Carbon Fibers[J]. Chinese Journal of Polymer Science, 2017, 35(6): 764-772.
Wei-wei Li, Kang Hong-liangKang, Jian Xu, 等. Effects of Ultra-high Temperature Treatment on the Microstructure of Carbon Fibers[J]. Chinese Journal of Polymer Science, 2017,35(6):764-772. DOI： 10.1007/s10118-017-1922-9.

Wei-wei Li, Kang Hong-liangKang, Jian Xu, et al. Effects of Ultra-high Temperature Treatment on the Microstructure of Carbon Fibers[J]. Chinese Journal of Polymer Science, 2017, 35(6): 764-772. DOI： 10.1007/s10118-017-1922-9.

摘要

Abstract

The microcrystalline structure and microvoid structure in carbon fibers during graphitization process (2300-2700 ℃) were characterized employing laser micro-Raman scattering (Raman)

X-ray diffraction (XRD)

small angle X-ray scattering (SAXS)

and high-resolution transmission electron microscopy (HR-TEM). The crystalline sizes (

) increased and interlayer spacing (

002

) decreased with increasing heat treatment temperature (HTT). The microvoids in the fibers grew up and contacted to the neighbors with the development of microcrystalline. In addition

the preferred orientation of graphite crystallite along fiber axis decreased and microvoids increased. The results are crucial for analyzing the evolution of microstructure of carbon fibers in the process of heat treatment and important for the preparation of high strength and high modulus carbon fibers.

关键词

Keywords

references

M.S.A. Rahaman , A.F. Ismail , A. Mustafa . . Polym. Degrad. Stab. , 2007 . 92 ( 8 ): 1421 DOI: 10.1016/j.polymdegradstab.2007.03.023 http://doi.org/10.1016/j.polymdegradstab.2007.03.023 .

D.D. Edie . . Carbon , 1998 . 36 ( 4 ): 345 DOI: 10.1016/S0008-6223(97)00185-1 http://doi.org/10.1016/S0008-6223(97)00185-1 .

A.J. Gao , C. Zhao , S. Luo , Y.J. Tong , L.H. Xu . . Mater. Lett. , 2011 . 65 ( 23-24 ): 3444 DOI: 10.1016/j.matlet.2011.07.057 http://doi.org/10.1016/j.matlet.2011.07.057 .

M.G. Dobb , H. Guo , D.J. Johnson , C.R. Park . . Carbon , 1995 . 33 ( 11 ): 1553 DOI: 10.1016/0008-6223(95)00114-S http://doi.org/10.1016/0008-6223(95)00114-S .

M.A. Montes-Moran , R.J. Young . . Carbon , 2002 . 40 ( 6 ): 845 DOI: 10.1016/S0008-6223(01)00212-3 http://doi.org/10.1016/S0008-6223(01)00212-3 .

M.A. Montes-Moran , R.J. Young . . Carbon , 2002 . 40 ( 6 ): 857 DOI: 10.1016/S0008-6223(01)00207-X http://doi.org/10.1016/S0008-6223(01)00207-X .

S.N. Chaudhuri , R.A. Chaudhuri , R.E. Benner , M.S. Penugonda . . Compos. Struct. , 2006 . 76 ( 4 ): 375 DOI: 10.1016/j.compstruct.2005.05.009 http://doi.org/10.1016/j.compstruct.2005.05.009 .

G.A. Zickler , B. Smarsly , N. Gierlinger , H. Peterlik , O. Paris . . Carbon , 2006 . 44 ( 15 ): 3239 DOI: 10.1016/j.carbon.2006.06.029 http://doi.org/10.1016/j.carbon.2006.06.029 .

G.H. Zhou , Y.Q. Liu , L.L. He , Q.G. Guo , H.Q. Ye . . Carbon , 2011 . 49 ( 9 ): 2883 DOI: 10.1016/j.carbon.2011.02.025 http://doi.org/10.1016/j.carbon.2011.02.025 .

A.F. Thunemann , W. Ruland . . Macromolecules , 2000 . 33 ( 5 ): 1848 DOI: 10.1021/ma991427x http://doi.org/10.1021/ma991427x .

C.Z. Zhu , X.F. Liu , X.L. Yu , N. Zhao , J.H. Liu , J. Xu . . Carbon , 2012 . 50 ( 1 ): 235 DOI: 10.1016/j.carbon.2011.08.040 http://doi.org/10.1016/j.carbon.2011.08.040 .

K. Fukuyama , Y. Kasahara , N. Kasahara , A. Oya , K. Nishikawa . . Carbon , 2001 . 39 ( 2 ): 287 DOI: 10.1016/S0008-6223(00)00159-7 http://doi.org/10.1016/S0008-6223(00)00159-7 .

M. Kaburagi , Y.Z. Bin , D. Zhu , C.Y. Xu , M. Matsuo . . Carbon , 2003 . 41 ( 5 ): 915 DOI: 10.1016/S0008-6223(02)00407-4 http://doi.org/10.1016/S0008-6223(02)00407-4 .

C.Z. Zhu , X.L. Yu , X.F. Liu , Y.Z. Mao , R.G. Liu , N. Zhao , X.L. Zhang , J. Xu . . Chinese J. Polym. Sci. , 2013 . 31 ( 5 ): 823 DOI: 10.1007/s10118-013-1272-1 http://doi.org/10.1007/s10118-013-1272-1 .

A. Takaku , M. Shioya . . J. Mater. Sci. , 1986 . 21 ( 12 ): 4443 DOI: 10.1007/BF01106569 http://doi.org/10.1007/BF01106569 .

T.C. Chieu , M.S. Dresselhaus , M. Endo . . Phys. Rev. B , 1982 . 26 ( 10 ): 5867 DOI: 10.1103/PhysRevB.26.5867 http://doi.org/10.1103/PhysRevB.26.5867 .

S.S. Tzeng . . Carbon , 2006 . 44 ( 10 ): 1986 DOI: 10.1016/j.carbon.2006.01.024 http://doi.org/10.1016/j.carbon.2006.01.024 .

F. Tuinstra , J.L. Koenig . . J. Compos. Mater. , 1970 . 4 ( 4 ): 492 .

H.S. Shim , R.H. Hurt , N.Y.C. Yang . . Carbon , 2000 . 38 ( 1 ): 29 DOI: 10.1016/S0008-6223(99)00096-2 http://doi.org/10.1016/S0008-6223(99)00096-2 .

浏览量

Downloads

CSCD

文章被引用时，请邮件提醒。

Submit

工具集

关联资源

Highly Conductive Ag/pCF/MVQ Composite Rubber for Efficient Electromagnetic Interference Shielding

Interfacial Improvement of Carbon Fiber/Epoxy Composites by Incorporating Superior and Versatile Multiscale Gradient Modulus Intermediate Layer with Rigid-flexible Hierarchical Structure

Highly Regio- and trans-Selective Ring-opening Metathesis Polymerization of Chiral Aza-norbornene with a Simple Phenylimido-Tungsten Catalyst

Upgrading Commercially Available Polyethylene to High-value Materials with Strong Mechanical Performance and Hydrophilicity by Blending with Ethylene/meta-Methoxystyrene Copolymers

Energy Storage Performance of Supercapacitors with Polyelectrolyte Surface Coatings: Effects of Dielectric Contrast