Antibacterial behaviour of quaternized poly(vinyl chloride)-<i>g</i>-poly(4-vinyl pyridine) graft copolymers

Madhumita Patel; Rajkumar Patel; Won Seok Chi; Jong Hak Kim; Jung-Suk Sung

doi:10.1007/s10118-015-1577-3

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Antibacterial behaviour of quaternized poly(vinyl chloride)-g-poly(4-vinyl pyridine) graft copolymers

PAPER | Updated：2022-01-17

- Antibacterial behaviour of quaternized poly(vinyl chloride)-g-poly(4-vinyl pyridine) graft copolymers
- Antibacterial Behaviour of Quaternized Poly(vinyl chloride)-g-Poly(4-vinyl pyridine) Graft Copolymers
- Chinese Journal of Polymer Science 2015年33卷第2期页码：265-274
- Affiliations：
  
  a.Department of Life Science, Dongguk University-Seoul, 3-26 Phil-dong, Chung-gu, Seoul 100-715, South Korea
  b.Department of Chemical and Biomolecular Engineering, Yonsei University, 262 Seongsanno, Seodaemun-gu, Seoul 120-749, South Korea
  c.Department of Chemistry and Nano Science, EwhaWomans University, Global Top 5 Research Program, 52 Ewhayeodae-gil, Seodaemun-gu, Seoul, 120-750, Korea
- Author bio：
  
  **Rajkumar Patel, E-mail: patelrajku@gmail.com
  Jong Hak Kim, E-mail: jonghak@yonsei.ac.kr
  Jung-Suk Sung, E-mail: sungjs@dongguk.edu
- Funds：
  
  National Research Foundation (NRF) grant funded by the Korean government (MEST) through the Core Research Program(2012R1A2A2A02011268);Agriculture Research Center program of Ministry for Food, Agriculture, Forestry, and Fisheries(IPET 112051-3);Korea CCS R&D Center and the Energy Efficiency & Resources of the Korea Institute of Energy Technology Evaluation and Planning (KETEP) grant funded by the Ministry of Knowledge Economy(20122010100040)
- DOI：10.1007/s10118-015-1577-3
  中图分类号：
- 收稿：2014-04-14，
  
  修回：2014-06-22，
  
  录用：2014-07-02，
  
  纸质出版：2015-02
- Accepted：
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Madhumita Patel, Rajkumar Patel, Won Seok Chi, 等. Antibacterial behaviour of quaternized poly(vinyl chloride)-g-poly(4-vinyl pyridine) graft copolymers[J]. Chinese Journal of Polymer Science, 2015,33(2):265-274. DOI: 10.1007/s10118-015-1577-3.

Madhumita Patel, Rajkumar Patel, Won Seok Chi, et al. Antibacterial Behaviour of Quaternized Poly(vinyl chloride)-g-Poly(4-vinyl pyridine) Graft Copolymers[J]. Chinese Journal of Polymer Science, 2015, 33(2): 265-274. DOI: 10.1007/s10118-015-1577-3.
Madhumita Patel, Rajkumar Patel, Won Seok Chi, 等. Antibacterial behaviour of quaternized poly(vinyl chloride)-g-poly(4-vinyl pyridine) graft copolymers[J]. Chinese Journal of Polymer Science, 2015,33(2):265-274. DOI: 10.1007/s10118-015-1577-3. DOI：

Madhumita Patel, Rajkumar Patel, Won Seok Chi, et al. Antibacterial Behaviour of Quaternized Poly(vinyl chloride)-g-Poly(4-vinyl pyridine) Graft Copolymers[J]. Chinese Journal of Polymer Science, 2015, 33(2): 265-274. DOI: 10.1007/s10118-015-1577-3. DOI：

摘要

Abstract

Amphiphilic graft copolymers consisting of poly(vinyl chloride) (PVC) main chains and poly(4-vinyl pyridine) (P4VP) side chains were synthesized

via

atom transfer radical polymerization (ATRP) using direct initiation of chlorine atoms. The successful synthesis of PVC-g-P4VP graft copolymers was confirmed by Fourier transform infrared spectroscopy (FTIR) and proton nuclear magnetic resonance (

H-NMR). Transmission electron microscope (TEM) and small angle X-ray scattering (SAXS) analysis showed that PVC-g-P4VP exhibited microphase-separated

ordered structure with 37.6 nm of domain spacing

which was not observed in neat PVC. For antibacterial applications

the tertiary nitrogen atoms of PVC-

-P4VP was quaternized using 1-bromohexane

as confirmed by FTIR measurements. Bacteria including

Escherichia coli

(

E. coli

)

Staphylococcus aureus

(

S. aureus

)

Bacillus cereus

(

B. cereus

)

and

Pseudomonas aeruginosa

(

P. aeruginosa

) were completely killed in 24 h on the quaternized PVC-g-P4VP (46% grafting) surface

indicating its excellent antibacterial behavior while it showed to be cytotoxic to mammalian cell.

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Antibacterial behaviour of quaternized poly(vinyl chloride)-g-poly(4-vinyl pyridine) graft copolymers

Antibacterial Behaviour of Quaternized Poly(vinyl chloride)-g-Poly(4-vinyl pyridine) Graft Copolymers

DOI：10.1007/s10118-015-1577-3

摘要

Abstract

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Keywords

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