Synthesis and MALDI-TOF Characterization of -CD Core ATRP Initiators and RAFT Chain Transfers with Different Degrees of Substitution

Yan Xin; Hong Wang; Bo-wen Liu; Jin-ying Yuan

doi:10.1007/s10118-015-1572-8

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Synthesis and MALDI-TOF Characterization of -CD Core ATRP Initiators and RAFT Chain Transfers with Different Degrees of Substitution

PAPER | Updated：2021-06-21

- Synthesis and MALDI-TOF Characterization of -CD Core ATRP Initiators and RAFT Chain Transfers with Different Degrees of Substitution
- Synthesis and MALDI-TOF Characterization of β-CD Core ATRP Initiators and RAFT Chain Transfers with Different Degrees of Substitution
- Chinese Journal of Polymer Science 2015年33卷第1期页码：36-48
- Affiliations：
  
  Key Lab of Organic Optoelectronics and Molecular Engineering of Ministry of Education, Department of Chemistry, Tsinghua University, Beijing 100084, China
- Author bio：
  
  **Jin-ying Yuan (袁金颖), E-mail: yuanjy@mail.tsinghua.edu.cn
- Funds：
  
  National Natural Science Foundation of China(21174076;21374053)
- DOI：10.1007/s10118-015-1572-8
  中图分类号：
- 收稿：2014-03-17，
  
  修回：2014-04-20，
  
  录用：2014-05-04，
  
  纸质出版：2015-01
- Accepted：
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Yan Xin, Hong Wang, Bo-wen Liu, 等. Synthesis and MALDI-TOF Characterization of -CD Core ATRP Initiators and RAFT Chain Transfers with Different Degrees of Substitution[J]. Chinese Journal of Polymer Science, 2015,33(1):36-48.

Yan Xin, Hong Wang, Bo-wen Liu, et al. Synthesis and MALDI-TOF Characterization of β-CD Core ATRP Initiators and RAFT Chain Transfers with Different Degrees of Substitution[J]. Chinese Journal of Polymer Science, 2015, 33(1): 36-48. DOI: 10.1007/s10118-015-1572-8.
Yan Xin, Hong Wang, Bo-wen Liu, 等. Synthesis and MALDI-TOF Characterization of -CD Core ATRP Initiators and RAFT Chain Transfers with Different Degrees of Substitution[J]. Chinese Journal of Polymer Science, 2015,33(1):36-48. DOI： 10.1007/s10118-015-1572-8.

Yan Xin, Hong Wang, Bo-wen Liu, et al. Synthesis and MALDI-TOF Characterization of β-CD Core ATRP Initiators and RAFT Chain Transfers with Different Degrees of Substitution[J]. Chinese Journal of Polymer Science, 2015, 33(1): 36-48. DOI: 10.1007/s10118-015-1572-8. DOI：

摘要

Abstract

In this paper

three different kinds of

-CD derivatives were synthesized as atom transfer radical polymerization (ATRP) initiator or reversible addition-fragmentation chain transfer polymerization (RAFT) chain transfers. The degree of substitution for each derivative was carefully characterized through

H-NMR

C-NMR spectroscopy and matrix-assisted laser desorption/ionization time of flight mass spectrometry (MALDI-TOF-MS). The factors influencing the degree of substitution were discussed. Moreover

the comparison between ATRP and RAFT was shown in the polymerization of

-isopropyl acrylamide (NIPAM).

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