HYDROGEN-BONDING INDUCED CHANGE OF CRYSTALLIZATION BEHAVIOR OF POLY(BUTYLENE SUCCINATE) IN ITS MIXTURES WITH BISPHENOL A

Fa-liang Luo; Fa-hai Luo; Qian Xing; Xiu-qin Zhang; Hong-qiao Jiao; Min Yao; Chun-tao Luo; Du-jin Wang

doi:10.1007/s10118-013-1364-y

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HYDROGEN-BONDING INDUCED CHANGE OF CRYSTALLIZATION BEHAVIOR OF POLY(BUTYLENE SUCCINATE) IN ITS MIXTURES WITH BISPHENOL A

PAPER | Updated：2023-01-03

- HYDROGEN-BONDING INDUCED CHANGE OF CRYSTALLIZATION BEHAVIOR OF POLY(BUTYLENE SUCCINATE) IN ITS MIXTURES WITH BISPHENOL A
- HYDROGEN-BONDING INDUCED CHANGE OF CRYSTALLIZATION BEHAVIOR OF POLY(BUTYLENE SUCCINATE) IN ITS MIXTURES WITH BISPHENOL A
- Chinese Journal of Polymer Science 2013年31卷第12期页码：1685-1696
- Affiliations：
  
  a.Key Laboratory of Energy Resource and Chemical Engineering of Ningxia, Ningxia University, Yinchuan 750021, China
  b.Liupanshan High School of Ningxia, Yinchuan 750002, China
  c.Beijing National Laboratory for Molecular Sciences, CAS Key Laboratory of Engineering Plastics, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China
  d.Shenhua Ningxia Coal Industry Group, Yinchuan 750011, China
- Author bio：
  
  **Fa-liang Luo (罗发亮), E-mail: flluo@iccas.ac.cn
  Du-jin Wang (王笃金), E-mail: djwang@iccas.ac.cn
- Funds：
  
  National Natural Science Foundation of China(51063004;21264012);China National Funds for Distinguished Young Scientists(50925313)
- DOI：10.1007/s10118-013-1364-y
  中图分类号：
- 收稿：2013-01-07，
  
  修回：2013-02-06，
  
  录用：2013-02-21，
  
  纸质出版：2013-12
- Accepted：
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Fa-liang Luo, Fa-hai Luo, Qian Xing, 等. HYDROGEN-BONDING INDUCED CHANGE OF CRYSTALLIZATION BEHAVIOR OF POLY(BUTYLENE SUCCINATE) IN ITS MIXTURES WITH BISPHENOL A[J]. Chinese Journal of Polymer Science, 2013,31(12):1685-1696.

Fa-liang Luo, Fa-hai Luo, Qian Xing, et al. HYDROGEN-BONDING INDUCED CHANGE OF CRYSTALLIZATION BEHAVIOR OF POLY(BUTYLENE SUCCINATE) IN ITS MIXTURES WITH BISPHENOL A[J]. Chinese Journal of Polymer Science, 2013, 31(12): 1685-1696.
Fa-liang Luo, Fa-hai Luo, Qian Xing, 等. HYDROGEN-BONDING INDUCED CHANGE OF CRYSTALLIZATION BEHAVIOR OF POLY(BUTYLENE SUCCINATE) IN ITS MIXTURES WITH BISPHENOL A[J]. Chinese Journal of Polymer Science, 2013,31(12):1685-1696. DOI： 10.1007/s10118-013-1364-y.

Fa-liang Luo, Fa-hai Luo, Qian Xing, et al. HYDROGEN-BONDING INDUCED CHANGE OF CRYSTALLIZATION BEHAVIOR OF POLY(BUTYLENE SUCCINATE) IN ITS MIXTURES WITH BISPHENOL A[J]. Chinese Journal of Polymer Science, 2013, 31(12): 1685-1696. DOI： 10.1007/s10118-013-1364-y.

摘要

Abstract

In the present work

the blend of poly(butylene succinate) (PBS) and bisphenol A (BPA) was prepared by solution mixing

and the intermolecular interactions between the two components were characterized by a combination of nuclear magnetic resonance (NMR) and Fourier transform infrared spectroscopy (FTIR). The results showed that intermolecular hydrogen-bonding forms between the carbonyl group of PBS and phenol hydroxyl of BPA. With the increase of BPA content

more hydrogen bonds were formed. The effect of hydrogen bonding on the crystallization behavior of PBS was investigated by differential scanning calorimetry (DSC) and polarized optical microscopy (POM). The results showed that the overall isothermal crystallization kinetics and the spherulite growth rate of PBS decrease with the increase of BPA content

while the PBS spherulite size increases with BPA content.

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