SYNTHESIS AND CHARACTERISTICS OF A CHELATING RESIN AS AN EXTRACTANT AND CHROMOGENIC REAGENT OF HEAVY METAL IONS IN SOLID PHASE EXTRACTION

Tian-lin Zhang; Hui-min Ma; Jia-jia Wang; Cai-yan Zhu; Bing-bing Wang

doi:10.1007/s10118-013-1303-y

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SYNTHESIS AND CHARACTERISTICS OF A CHELATING RESIN AS AN EXTRACTANT AND CHROMOGENIC REAGENT OF HEAVY METAL IONS IN SOLID PHASE EXTRACTION

PAPER | Updated：2023-01-03

- SYNTHESIS AND CHARACTERISTICS OF A CHELATING RESIN AS AN EXTRACTANT AND CHROMOGENIC REAGENT OF HEAVY METAL IONS IN SOLID PHASE EXTRACTION
- SYNTHESIS AND CHARACTERISTICS OF A CHELATING RESIN AS AN EXTRACTANT AND CHROMOGENIC REAGENT OF HEAVY METAL IONS IN SOLID PHASE EXTRACTION
- Chinese Journal of Polymer Science 2013年31卷第8期页码：1108-1116
- Affiliations：
  
  a.Department of Chemical Engineering, Huaihai Institute of Technology, Lianyungang 222005, China
  b.School of Chemical Engineering & Technology, University of Mining and Technology, Xuzhou 221116, China
  c.College of Environment and Spatial Informatics, University of Mining and Technology, Xuzhou 221116, China
- Author bio：
  
  **Tian-lin Zhang (张田林), E-mail: zhangtianlin@hhit.edu.cn
- Funds：
  
  National Natural Science Foundation of China(50873042);Natural Science Foundation for Colleges and Universities of Jiangsu Province(11KJA430008)
- DOI：10.1007/s10118-013-1303-y
  中图分类号：
- 收稿：2012-09-17，
  
  修回：2012-11-13，
  
  录用：2012-11-21，
  
  纸质出版：2013-08
- Accepted：
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Tian-lin Zhang, Hui-min Ma, Jia-jia Wang, 等. SYNTHESIS AND CHARACTERISTICS OF A CHELATING RESIN AS AN EXTRACTANT AND CHROMOGENIC REAGENT OF HEAVY METAL IONS IN SOLID PHASE EXTRACTION[J]. Chinese Journal of Polymer Science, 2013,31(8):1108-1116.

Tian-lin Zhang, Hui-min Ma, Jia-jia Wang, et al. SYNTHESIS AND CHARACTERISTICS OF A CHELATING RESIN AS AN EXTRACTANT AND CHROMOGENIC REAGENT OF HEAVY METAL IONS IN SOLID PHASE EXTRACTION[J]. Chinese Journal of Polymer Science, 2013, 31(8): 1108-1116.
Tian-lin Zhang, Hui-min Ma, Jia-jia Wang, 等. SYNTHESIS AND CHARACTERISTICS OF A CHELATING RESIN AS AN EXTRACTANT AND CHROMOGENIC REAGENT OF HEAVY METAL IONS IN SOLID PHASE EXTRACTION[J]. Chinese Journal of Polymer Science, 2013,31(8):1108-1116. DOI： 10.1007/s10118-013-1303-y.

Tian-lin Zhang, Hui-min Ma, Jia-jia Wang, et al. SYNTHESIS AND CHARACTERISTICS OF A CHELATING RESIN AS AN EXTRACTANT AND CHROMOGENIC REAGENT OF HEAVY METAL IONS IN SOLID PHASE EXTRACTION[J]. Chinese Journal of Polymer Science, 2013, 31(8): 1108-1116. DOI： 10.1007/s10118-013-1303-y.

摘要

Abstract

A new chelating resin (CPS-DMA-SABA) was synthesized with the chloromethylated cross-linked polystyrene porous beads (CPS) as raw materials

which were bonded with salicylidene-o-aminobenzoic acid (SABA) on the surface via a quaternary ammonium unit as a linker. The results showed that CPS-DMA-SABA would easily change into a zwitterionic chelating resin (CPS-DMA-SABZ) when washed with distilled water. CPS-DMA-SABA was characterized by elemental analysis

infrared spectra and thermo-gravimetric analysis. The ion sorption capacities of CPS-DMA-SABA were found to be 1916 μg/g for Zn

with pH at 4.5

1620 μg/g for Cu

with pH at 6.2

1291 μg/g for Ni

with pH at 6.6 and 780 μg/g for Cr

with pH at 5.5

respectively. The experiments showed CPS-DMA-SABA also changed its color when meeting with the metal ion in the aqueous solution. As a consequence

CPS-DMA-SABA can not only be used as a solid phase extractant but also an indicator for confirming the heavy metal ion in solutions.

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