SYNTHESES AND CHARACTERIZATIONS OF OLIGO(AZOMETHINE ETHER)S DERIVED FROM 2,2′-[1,4-ENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE AND 2,2′-[1,2-PHENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE

İsmet Kaya; Süleyman Çulhaoğlu

doi:10.1007/s10118-012-1143-1

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SYNTHESES AND CHARACTERIZATIONS OF OLIGO(AZOMETHINE ETHER)S DERIVED FROM 2,2′-[1,4-ENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE AND 2,2′-[1,2-PHENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE

PAPER | Updated：2023-01-03

- SYNTHESES AND CHARACTERIZATIONS OF OLIGO(AZOMETHINE ETHER)S DERIVED FROM 2,2′-[1,4-ENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE AND 2,2′-[1,2-PHENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE
- SYNTHESES AND CHARACTERIZATIONS OF OLIGO(AZOMETHINE ETHER)S DERIVED FROM 2,2′-[1,4-ENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE AND 2,2′-[1,2-PHENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE
- Chinese Journal of Polymer Science 2012年30卷第5期页码：682-693
- Affiliations：
  
  Çanakkale Onsekiz Mart University, Faculty of Science and Arts, Department of Chemistry, Çanakkale 17020, Turkey
- Author bio：
  
  *İsmet Kaya, E-mail: kayaismet@hotmail.com
- Funds：
- DOI：10.1007/s10118-012-1143-1
  中图分类号：
- 收稿：2011-11-25，
  
  修回：2012-01-07，
  
  录用：2012-01-17，
  
  纸质出版：2012-09
- Accepted：
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İsmet Kaya, Süleyman Çulhaoğlu. SYNTHESES AND CHARACTERIZATIONS OF OLIGO(AZOMETHINE ETHER)S DERIVED FROM 2,2′-[1,4-ENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE AND 2,2′-[1,2-PHENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE[J]. Chinese Journal of Polymer Science, 2012,30(5):682-693.

İsmet Kaya, Süleyman Çulhaoğlu. SYNTHESES AND CHARACTERIZATIONS OF OLIGO(AZOMETHINE ETHER)S DERIVED FROM 2,2′-[1,4-ENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE AND 2,2′-[1,2-PHENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE[J]. Chinese Journal of Polymer Science, 2012, 30(5): 682-693.
İsmet Kaya, Süleyman Çulhaoğlu. SYNTHESES AND CHARACTERIZATIONS OF OLIGO(AZOMETHINE ETHER)S DERIVED FROM 2,2′-[1,4-ENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE AND 2,2′-[1,2-PHENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE[J]. Chinese Journal of Polymer Science, 2012,30(5):682-693. DOI： 10.1007/s10118-012-1143-1.

İsmet Kaya, Süleyman Çulhaoğlu. SYNTHESES AND CHARACTERIZATIONS OF OLIGO(AZOMETHINE ETHER)S DERIVED FROM 2,2′-[1,4-ENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE AND 2,2′-[1,2-PHENYLENEBIS(METHYLENEOXY)]DIBENZALDEHYDE[J]. Chinese Journal of Polymer Science, 2012, 30(5): 682-693. DOI： 10.1007/s10118-012-1143-1.

摘要

Abstract

The oligo(azomethine ether)s were synthesized

via

polycondensation of alkyl diamines with aromatic dialdehydes. Two series of dialdehydes

namely 2

2′-[1

2-phenylenebis(methyleneoxy)]dibenzaldehyde [2

2′-1

2-(PBMODB)]

and 2

2′-[1

4-phenylenebis(methyleneoxy)]dibenzaldehyde [2

2′-1

4-(PBMODB)]

were prepared from the condensation reactions of salicylaldehyde with o-xylenedibromide and p-xylenedibromide

respectively. The structures of dialdehydes and oligomers were determined by FT-IR

H-NMR and

C-NMR. The thermal analyses of oligomers were conducted by DSC and TG/DTA techniques

respectively. Size exclusion chromatography (SEC) technique was also used to determine molecular weights and molecular weight distributions of oligomers. Electrochemical properties of the synthesized products were investigated.

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