SYNTHESIS AND CHARACERIZATION OF LADDER-LIKE POLYDECYLSILSESQUIOXANE*

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SYNTHESIS AND CHARACERIZATION OF LADDER-LIKE POLYDECYLSILSESQUIOXANE*

Papers | Updated：2021-06-21

- SYNTHESIS AND CHARACERIZATION OF LADDER-LIKE POLYDECYLSILSESQUIOXANE*
- SYNTHESIS AND CHARACERIZATION OF LADDER-LIKE POLYDECYLSILSESQUIOXANE*
- 高分子科学（英文版） 1999年17卷第1期页码：71-74
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- 纸质出版：1999-02-20
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SYNTHESIS AND CHARACERIZATION OF LADDER-LIKE POLYDECYLSILSESQUIOXANE*[J]. 高分子科学（英文版）, 1999,17(1):71-74.

SYNTHESIS AND CHARACERIZATION OF LADDER-LIKE POLYDECYLSILSESQUIOXANE*[J]. 1999, 17(1): 71-74.
SYNTHESIS AND CHARACERIZATION OF LADDER-LIKE POLYDECYLSILSESQUIOXANE*[J]. 高分子科学（英文版）, 1999,17(1):71-74. DOI：

SYNTHESIS AND CHARACERIZATION OF LADDER-LIKE POLYDECYLSILSESQUIOXANE*[J]. 1999, 17(1): 71-74. DOI：

摘要

Ladder-like polydecylsilsesquioxane (LPDS) was synthesized by a preamminolysis reaction ofdecyltrichlorosilane with ethylene diamine

followed by hydrolysis and polycondensation reaction. LPDS issoluble in a nonpolar solvent such as heptane and insoluble in a high polar solvent such as methanol. It wascharaterized by IR

1H-NMR

29Si-NMR

GPC and X-ray diffraction.

Abstract

Ladder-like polydecylsilsesquioxane (LPDS) was synthesized by a preamminolysis reaction ofdecyltrichlorosilane with ethylene diamine

followed by hydrolysis and polycondensation reaction. LPDS issoluble in a nonpolar solvent such as heptane and insoluble in a high polar solvent such as methanol. It wascharaterized by IR

1H-NMR

29Si-NMR

GPC and X-ray diffraction.

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