SYNTHESIS AND POLYMERIZATION OF 2-OXO-3-METHYLENE-1,4-DIOXANES

FENG Pinzhen; WANG Aiwen

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SYNTHESIS AND POLYMERIZATION OF 2-OXO-3-METHYLENE-1,4-DIOXANES

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- SYNTHESIS AND POLYMERIZATION OF 2-OXO-3-METHYLENE-1,4-DIOXANES
- SYNTHESIS AND POLYMERIZATION OF 2-OXO-3-METHYLENE-1,4-DIOXANES
- 高分子科学（英文版） 1991年9卷第3期页码：220-225
- Affiliations：
  
  1. Chemistry Department, Graduate School, Academia Sinica,Beijing
  2.   Graduate School
  3.   Academia Sinica
  4.   Beijing
- Author bio：
- Funds：
- DOI：
  中图分类号：
- 纸质出版：1991-09-20
- Accepted：
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[1]冯品珍,王爱文.SYNTHESIS AND POLYMERIZATION OF 2-OXO-3-METHYLENE-1,4-DIOXANES[J].Chinese Journal of Polymer Science,1991,{4}(03):220-225.

FENG Pinzhen, WANG Aiwen. SYNTHESIS AND POLYMERIZATION OF 2-OXO-3-METHYLENE-1,4-DIOXANES[J]. 1991, 9(3): 220-225.
[1]冯品珍,王爱文.SYNTHESIS AND POLYMERIZATION OF 2-OXO-3-METHYLENE-1,4-DIOXANES[J].Chinese Journal of Polymer Science,1991,{4}(03):220-225. DOI：

FENG Pinzhen, WANG Aiwen. SYNTHESIS AND POLYMERIZATION OF 2-OXO-3-METHYLENE-1,4-DIOXANES[J]. 1991, 9(3): 220-225. DOI：

摘要

正

A new kind of monomers was successfully synthesized by the reaction between 2-chloro methyl cycloketal and trimethylsilyl cyanide

followed by ring closure and dehaiogenation. Polymerizations of the monomers were carried out in benzene solution at 80℃with benzoyl peroxide as initiator. Both the structures of monomers and polymers were characterized by IR

H NMR

C NMR and elemental analysis.

Abstract

A new kind of monomers was successfully synthesized by the reaction between 2-chloro methyl cycloketal and trimethylsilyl cyanide

followed by ring closure and dehaiogenation. Polymerizations of the monomers were carried out in benzene solution at 80℃ with benzoyl peroxide as initiator. Both the structures of monomers and polymers were characterized by IR

H NMR

C NMR and elemental analysis.

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