<正> The compositional homogeneity of a poly (ethylene terephthalate)-poly (tetramethylene ether) multiblock copolymer sample with low content of hard segment was examined by GPC
TLC
and solubility method. The copolymer sample was found to have a uniform composition as a function of elution volume over the major portion of sample from GPC method. However within one elution fraction
the copolymer chains
although having the same hydrodynamic volume
may have some difference in composition. Two fractions with different composition were obtained by precipitation in ethanol. Some low molar mass copolymers were also separated by a TLC technique from the copolymer sample.
Abstract
The compositional homogeneity of a poly (ethylene terephthalate)-poly (tetramethylene ether) multiblock copolymer sample with low content of hard segment was examined by GPC
TLC
and solubility method. The copolymer sample was found to have a uniform composition as a function of elution volume over the major portion of sample from GPC method. However within one elution fraction
the copolymer chains
although having the same hydrodynamic volume
may have some difference in composition. Two fractions with different composition were obtained by precipitation in ethanol. Some low molar mass copolymers were also separated by a TLC technique from the copolymer sample.
关键词
Keywords
references
The trial reading is over, you can activate your VIP account to continue reading.