Thermally Conductive and Insulating Epoxy Composites by Synchronously Incorporating Si-sol Functionalized Glass Fibers and Boron Nitride Fillers

Rui-Han Zhang; Xue-Tao Shi; Lin Tang; Zheng Liu; Jun-Liang Zhang; Yong-Qiang Guo; Jun-Wei Gu

doi:10.1007/s10118-020-2391-0

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Thermally Conductive and Insulating Epoxy Composites by Synchronously Incorporating Si-sol Functionalized Glass Fibers and Boron Nitride Fillers

ARTICLE | Updated：2020-03-17

- Thermally Conductive and Insulating Epoxy Composites by Synchronously Incorporating Si-sol Functionalized Glass Fibers and Boron Nitride Fillers
- Chinese Journal of Polymer Science Vol. 38, Issue 7, Pages: 730-739(2020)
- Affiliations：
  
  Shaanxi Key Laboratory of Macromolecular Science and Technology, School of Chemistry and Chemical Engineering, Northwestern Polytechnical University, Xi’an 710072, China
- Author bio：
  
  gjw@nwpu.edu.cn or nwpugjw@163.com
- Funds：
- DOI：10.1007/s10118-020-2391-0
  CLC：
- Received：14 December 2019，
  
  Revised：2020-1-9，
  
  Accepted：15 January 2020，
  
  Online First：17 March 2020，
  
  Published：2020-07
- Accepted：
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Zhang, R. H.; Shi, X. T.; Tang, L.; Liu, Z.; Zhang, J. L.; Guo, Y. Q.; Gu, J. W. Thermally conductive and insulating epoxy composites by synchronously incorporating Si-sol functionalized glass fibers and boron nitride fillers. Chinese J. Polym. Sci. 2020, 38, 730–739

Rui-Han Zhang, Xue-Tao Shi, Lin Tang, et al. Thermally Conductive and Insulating Epoxy Composites by Synchronously Incorporating Si-sol Functionalized Glass Fibers and Boron Nitride Fillers[J]. Chinese Journal of Polymer Science, 2020, 38(7): 730-739.
Zhang, R. H.; Shi, X. T.; Tang, L.; Liu, Z.; Zhang, J. L.; Guo, Y. Q.; Gu, J. W. Thermally conductive and insulating epoxy composites by synchronously incorporating Si-sol functionalized glass fibers and boron nitride fillers. Chinese J. Polym. Sci. 2020, 38, 730–739 DOI： 10.1007/s10118-020-2391-0.

Rui-Han Zhang, Xue-Tao Shi, Lin Tang, et al. Thermally Conductive and Insulating Epoxy Composites by Synchronously Incorporating Si-sol Functionalized Glass Fibers and Boron Nitride Fillers[J]. Chinese Journal of Polymer Science, 2020, 38(7): 730-739. DOI： 10.1007/s10118-020-2391-0.

摘要

Abstract

Glass fibers (GFs)/epoxy laminated composites always present weak interlaminar shear strength (ILSS) and low cross-plane thermal conductivity coefficient (

┴

). In this work

silica-sol

synthesized from tetraethyl orthosilicate (TEOS) and KH-560

via

sol-gel method

was employed to functionalize the surface of GFs (Si-GFs). Together with a spherical boron nitride (BNN-30)

the thermally conductive BNN-30/Si-GFs/epoxy laminated composites were then fabricated. Results demonstrate that Si-sol is beneficial to the improvement of mechanical properties for epoxy laminated composites (especially for ILSS). The BNN-30/Si-GFs/epoxy laminated composites with 15 wt% BNN-30 fillers display the optimal comprehensive properties. In-plane

(

) and

┴

reach the maximum of 2.37 and 1.07 W·m

−1

·K

−1

146.9% and 132.6% higher than those of Si-GFs/epoxy laminated composites (

= 0.96 W·m

−1

·K

−1

and

┴

= 0.46 W·m

−1

·K

−1

)

respectively

and also about 10.8 and 4.9 times those of pure epoxy resin (

┴

0.22 W·m

−1

·K

−1

). And the heat-resistance index (

HRI

)

dielectric constant (

)

dielectric loss (tan

)

breakdown strength (

)

surface resistivity (

) as well as volume resistivity (

) are 197.3 °C

4.95

0.0046

22.3 kV·mm

−1

1.8 × 10

and 2.1 × 10

Ω·cm

respectively.

关键词

Keywords

references

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