Superhydrophobic PVDF/TiO<sub>2</sub>-SiO<sub>2</sub> Membrane with Hierarchical Roughness in Membrane Distillation for Water Recovery from Phenolic Rich Solution Containing Surfactant

N. Hamzah; C. P. Leo; B. S. Ooi

doi:10.1007/s10118-019-2235-y

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Superhydrophobic PVDF/TiO₂-SiO₂ Membrane with Hierarchical Roughness in Membrane Distillation for Water Recovery from Phenolic Rich Solution Containing Surfactant

ARTICLE | Updated：2021-02-18

- Superhydrophobic PVDF/TiO₂-SiO₂ Membrane with Hierarchical Roughness in Membrane Distillation for Water Recovery from Phenolic Rich Solution Containing Surfactant
- Chinese Journal of Polymer Science Vol. 37, Issue 6, Pages: 609-616(2019)
- Affiliations：
  
  School of Chemical Engineering, Engineering Campus, Universiti Sains Malaysia, 14300 Nibong Tebal, Penang, Malaysia
- Author bio：
  
  chcpleo@usm.my
- Funds：
- DOI：10.1007/s10118-019-2235-y
  CLC：
- Received：19 October 2018，
  
  Revised：2019-1-18，
  
  Accepted：28 January 2019，
  
  Online First：14 March 2019，
  
  Published：2019-06
- Accepted：
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Citation: Hamzah, N.; Leo, C. P.; Ooi, B. S. Superhydrophobic PVDF/TiO₂-SiO₂ membrane with hierarchical roughness in membrane distillation for water recovery from phenolic rich solution containing surfactant. Chinese J. Polym. Sci. 2019, 37, 609–616 DOI: 10.1007/s10118-019-2235-y.

N. Hamzah, C. P. Leo, B. S. Ooi. Superhydrophobic PVDF/TiO₂-SiO₂ Membrane with Hierarchical Roughness in Membrane Distillation for Water Recovery from Phenolic Rich Solution Containing Surfactant[J]. Chinese Journal of Polymer Science, 2019, 37(6): 609-616. DOI: 10.1007/s10118-019-2235-y.
Citation: Hamzah, N.; Leo, C. P.; Ooi, B. S. Superhydrophobic PVDF/TiO₂-SiO₂ membrane with hierarchical roughness in membrane distillation for water recovery from phenolic rich solution containing surfactant. Chinese J. Polym. Sci. 2019, 37, 609–616 DOI: 10.1007/s10118-019-2235-y. DOI：

N. Hamzah, C. P. Leo, B. S. Ooi. Superhydrophobic PVDF/TiO₂-SiO₂ Membrane with Hierarchical Roughness in Membrane Distillation for Water Recovery from Phenolic Rich Solution Containing Surfactant[J]. Chinese Journal of Polymer Science, 2019, 37(6): 609-616. DOI: 10.1007/s10118-019-2235-y. DOI：

摘要

Abstract

Superhydrophobic poly(vinylidene fluoride) (PVDF) membrane incorporated with nanoparticles was applied in membrane distillation to recover water from phenolic rich solution containing surfactant. The membranes coated on woven support were fabricated using phase inversion with dual bath coagulation and post-modified using silane. The membranes incorporated with TiO

SiO

or a mixture of TiO

-SiO

nanoparticles achieved the water contact angle higher than 160°. The addition of TiO

-SiO

mixture into PVDF matrix further enhanced the hierarchical roughness of membrane. Hence

PVDF/TiO

-SiO

membrane achieved the highest permeation flux and rejected 99.9% of gallic acid in the feed (100 g/L). PVDF/TiO

-SiO

membrane also maintained a relative flux (

) higher than 0.9 after 8 h of operation. Even with the presence of surfactant in phenolic rich solution

PVDF/TiO

-SiO

membrane was able to exhibit relative flux above 0.8. The significant changes on the hydrophobicity and chemical properties of PVDF/TiO

-SiO

membrane due to fouling were not observed after 50 h of static adsorption test.

关键词

Keywords

references

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Superhydrophobic PVDF/TiO2-SiO2 Membrane with Hierarchical Roughness in Membrane Distillation for Water Recovery from Phenolic Rich Solution Containing Surfactant

DOI：10.1007/s10118-019-2235-y

摘要

Abstract

关键词

Keywords

references

Superhydrophobic PVDF/TiO₂-SiO₂ Membrane with Hierarchical Roughness in Membrane Distillation for Water Recovery from Phenolic Rich Solution Containing Surfactant