Synthesis and AO Resistant Properties of Novel Polyimide Fibers Containing Phenylphosphine Oxide Groups in Main Chain

Yong Zhao; Hong Gao; Guo-Min Li; Fang-Fang Liu; Xue-Min Dai; Zhi-Xin Dong; Xue-Peng Qiu

doi:10.1007/s10118-019-2179-2

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Synthesis and AO Resistant Properties of Novel Polyimide Fibers Containing Phenylphosphine Oxide Groups in Main Chain

ARTICLE | Updated：2021-02-18

- Synthesis and AO Resistant Properties of Novel Polyimide Fibers Containing Phenylphosphine Oxide Groups in Main Chain
- Chinese Journal of Polymer Science Vol. 37, Issue 1, Pages: 59-67(2019)
- Affiliations：
  
  a.Polymer Composites Engineering Laboratory, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China
  b.University of Chinese Academy of Sciences, Beijing 100049, China
  c.China Academy of Space Technology, Beijing 100094, China
- Author bio：
  
  zxdong@ciac.ac.cn (Z.X.D.)
  xp_q@ciac.ac.cn (X.P.Q.)
- Funds：
- DOI：10.1007/s10118-019-2179-2
  CLC：
- Received：06 June 2018，
  
  Revised：2018-7-21，
  
  Accepted：06 August 2018，
  
  Online First：07 September 2018，
  
  Published：2019-01
- Accepted：
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Citation: Zhao, Y.; Gao, H.; Li, G. M.; Liu, F. F.; Dai, X. M.; Dong, Z. X.; Qiu, X. P. Synthesis and AO resistant properties of novel polyimide fibers containing phenylphosphine oxide groups in main chain. Chinese J. Polym. Sci. 2019, 37, 59–67

Yong Zhao, Hong Gao, Guo-Min Li, et al. Synthesis and AO Resistant Properties of Novel Polyimide Fibers Containing Phenylphosphine Oxide Groups in Main Chain[J]. Chinese Journal of Polymer Science, 2019, 37(1): 59-67.
Citation: Zhao, Y.; Gao, H.; Li, G. M.; Liu, F. F.; Dai, X. M.; Dong, Z. X.; Qiu, X. P. Synthesis and AO resistant properties of novel polyimide fibers containing phenylphosphine oxide groups in main chain. Chinese J. Polym. Sci. 2019, 37, 59–67 DOI： 10.1007/s10118-019-2179-2.

Yong Zhao, Hong Gao, Guo-Min Li, et al. Synthesis and AO Resistant Properties of Novel Polyimide Fibers Containing Phenylphosphine Oxide Groups in Main Chain[J]. Chinese Journal of Polymer Science, 2019, 37(1): 59-67. DOI： 10.1007/s10118-019-2179-2.

摘要

Abstract

A series of co-polyimide (PI) fibers containing phenylphosphine oxide (PPO) group were synthesized by incorporating the bis(4-aminophenoxy) phenyl phosphine oxide (DAPOPPO) monomer into the PI molecular chain followed by dry-jet wet spinning. The effects of DAPOPPO molar content on the atomic oxygen (AO) resistance of the fibers were investigated systematically. When the AO fluence increased from 0 atoms·cm

−2

to 3.2 × 10

atoms·cm

−2

the mass loss of the fibers showed the dependence on DAPOPPO molar content in co-PI fibers. The PI fiber containing 40% DAPOPPO showed lower mass loss compared to those containing 0% and 20% DAPOPPO. At higher AO fluence

the higher DAPOPPO content gave rise to dense carpet-like surface of fibers. XPS results indicated that the passivated phosphate layer was deposited on the fiber surface when exposed to AO

which effectively prevented fiber from AO erosion. With the DAPOPPO content increasing from 0% to 40%

the retentions of tensile strength and initial modulus for the fibers exhibited obvious growth from 44% to 68%

and 59% to 70%

after AO exposure with the fluence of 3.2 × 10

atoms·cm

−2

. The excellent AO resistance benefits the fibers for application in low Earth orbit as flexible construction components.

关键词

Keywords

references

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