Preparation and Properties of Poly(aryl ether sulfone ketone) Ultrafiltration Membrane Containing Fluorene Group for High Temperature Condensed Water Treatment

Xiang-Li Meng; Gen-Hua Yu; Jian Ma

doi:10.1007/s10118-018-2142-7

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Preparation and Properties of Poly(aryl ether sulfone ketone) Ultrafiltration Membrane Containing Fluorene Group for High Temperature Condensed Water Treatment

ARTICLE | Updated：2021-02-18

- Preparation and Properties of Poly(aryl ether sulfone ketone) Ultrafiltration Membrane Containing Fluorene Group for High Temperature Condensed Water Treatment
- Chinese Journal of Polymer Science Vol. 36, Issue 8, Pages: 970-978(2018)
- Affiliations：
  
  School of Chemistry and Chemical Engineering, Harbin Institute of Technology, Harbin 150001, China
- Author bio：
  
  mengxl2009@hit.edu.cn
- Funds：
- DOI：10.1007/s10118-018-2142-7
  CLC：
- Received：13 March 2017，
  
  Revised：2018-4-5，
  
  Accepted：07 April 2018，
  
  Online First：11 May 2018，
  
  Published：2018-08
- Accepted：
Scan QR Code
Xiang-Li Meng, Gen-Hua Yu, Jian Ma. Preparation and Properties of Poly(aryl ether sulfone ketone) Ultrafiltration Membrane Containing Fluorene Group for High Temperature Condensed Water Treatment[J]. Chinese Journal of Polymer Science, 2018, 36(8): 970-978.
DOI：

Xiang-Li Meng, Gen-Hua Yu, Jian Ma. Preparation and Properties of Poly(aryl ether sulfone ketone) Ultrafiltration Membrane Containing Fluorene Group for High Temperature Condensed Water Treatment[J]. Chinese Journal of Polymer Science, 2018, 36(8): 970-978. DOI： 10.1007/s10118-018-2142-7.

摘要

Abstract

Novel poly(aryl ether sulfone ketone)s (PAESK) were synthesized from bisphenol A (BPA)

9′-bis(4-hydroxyphenyl) fluorene (BHPF)

4′-dichlorodiphenylsulfone (DCS) and 4

4′-difluorobenzophenone (DFB)

via

nucleophilic substitution polymerization

which were subsequently used to fabricate ultrafiltration membrane by phase-inversion method for high temperature condensed water treatment. The obtained high molecular weight co-polymers with fluorene group with good solubility and good thermal stability

can be easily cast into flexible

white and non-transparent flat films. The influence of molar ratio of BPA and BHPF on the properties of the prepared co-polymers and membranes was investigated in detail. SEM study of the morphology of the membranes indicated that the prepared membranes possessed homogeneous pores on the top surface and were sponge-like or finger-like in cross-section. Pure water flux of the membranes increased from 71.87 L·m

−2

·h

−1

to 247.65 L·m

−2

·h

−1

while the retention of BSA decreased slightly

and the water contact angle decreased from 82.1° to 55.6° with the PVP concentration from 0 wt% to 10 wt%. With increasing concentration of PVP

the mechanical properties of membranes decreased

while the thermal stability increased. The permeate flux measurement showed that the PAESK membrane had the potential for high temperature condensed water treatment.

关键词

Keywords

references

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