Effects of Ultra-high Temperature Treatment on the Microstructure of Carbon Fibers

Wei-wei Li; Kang Hong-liangKang; Jian Xu; Rui-gang Liu

doi:10.1007/s10118-017-1922-9

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Effects of Ultra-high Temperature Treatment on the Microstructure of Carbon Fibers

Papers | Updated：2021-02-18

- Effects of Ultra-high Temperature Treatment on the Microstructure of Carbon Fibers
- Chinese Journal of Polymer Science Vol. 35, Issue 6, Pages: 764-772(2017)
- Affiliations：
  
  a.Laboratory of Polymer Physics and Chemistry, Beijing National Laboratory for Molecular Science, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100190, China
  b.University of Chinese Academy of Sciences, Beijing 100049, China
- Author bio：
  
  Jian Xu (徐坚), E-mail: jxu@iccas.ac.cn
  Rui-gang Liu (刘瑞刚), E-mail: rgliu@iccas.ac.cn
- Funds：
- DOI：10.1007/s10118-017-1922-9
  CLC：
- Received：18 September 2016，
  
  Revised：2016-11-30，
  
  Accepted：02 December 2016，
  
  Published：05 June 2017
- Accepted：
Scan QR Code
Wei-wei Li, Kang Hong-liangKang, Jian Xu, et al. Effects of Ultra-high Temperature Treatment on the Microstructure of Carbon Fibers[J]. Chinese Journal of Polymer Science, 2017, 35(6): 764-772.
DOI：

Wei-wei Li, Kang Hong-liangKang, Jian Xu, et al. Effects of Ultra-high Temperature Treatment on the Microstructure of Carbon Fibers[J]. Chinese Journal of Polymer Science, 2017, 35(6): 764-772. DOI： 10.1007/s10118-017-1922-9.

摘要

Abstract

The microcrystalline structure and microvoid structure in carbon fibers during graphitization process (2300-2700 ℃) were characterized employing laser micro-Raman scattering (Raman)

X-ray diffraction (XRD)

small angle X-ray scattering (SAXS)

and high-resolution transmission electron microscopy (HR-TEM). The crystalline sizes (

) increased and interlayer spacing (

002

) decreased with increasing heat treatment temperature (HTT). The microvoids in the fibers grew up and contacted to the neighbors with the development of microcrystalline. In addition

the preferred orientation of graphite crystallite along fiber axis decreased and microvoids increased. The results are crucial for analyzing the evolution of microstructure of carbon fibers in the process of heat treatment and important for the preparation of high strength and high modulus carbon fibers.

关键词

Keywords

references

M.S.A. Rahaman , A.F. Ismail , A. Mustafa . . Polym. Degrad. Stab. , 2007 . 92 ( 8 ): 1421 DOI: 10.1016/j.polymdegradstab.2007.03.023 http://doi.org/10.1016/j.polymdegradstab.2007.03.023 .

D.D. Edie . . Carbon , 1998 . 36 ( 4 ): 345 DOI: 10.1016/S0008-6223(97)00185-1 http://doi.org/10.1016/S0008-6223(97)00185-1 .

A.J. Gao , C. Zhao , S. Luo , Y.J. Tong , L.H. Xu . . Mater. Lett. , 2011 . 65 ( 23-24 ): 3444 DOI: 10.1016/j.matlet.2011.07.057 http://doi.org/10.1016/j.matlet.2011.07.057 .

M.G. Dobb , H. Guo , D.J. Johnson , C.R. Park . . Carbon , 1995 . 33 ( 11 ): 1553 DOI: 10.1016/0008-6223(95)00114-S http://doi.org/10.1016/0008-6223(95)00114-S .

M.A. Montes-Moran , R.J. Young . . Carbon , 2002 . 40 ( 6 ): 845 DOI: 10.1016/S0008-6223(01)00212-3 http://doi.org/10.1016/S0008-6223(01)00212-3 .

M.A. Montes-Moran , R.J. Young . . Carbon , 2002 . 40 ( 6 ): 857 DOI: 10.1016/S0008-6223(01)00207-X http://doi.org/10.1016/S0008-6223(01)00207-X .

S.N. Chaudhuri , R.A. Chaudhuri , R.E. Benner , M.S. Penugonda . . Compos. Struct. , 2006 . 76 ( 4 ): 375 DOI: 10.1016/j.compstruct.2005.05.009 http://doi.org/10.1016/j.compstruct.2005.05.009 .

G.A. Zickler , B. Smarsly , N. Gierlinger , H. Peterlik , O. Paris . . Carbon , 2006 . 44 ( 15 ): 3239 DOI: 10.1016/j.carbon.2006.06.029 http://doi.org/10.1016/j.carbon.2006.06.029 .

G.H. Zhou , Y.Q. Liu , L.L. He , Q.G. Guo , H.Q. Ye . . Carbon , 2011 . 49 ( 9 ): 2883 DOI: 10.1016/j.carbon.2011.02.025 http://doi.org/10.1016/j.carbon.2011.02.025 .

A.F. Thunemann , W. Ruland . . Macromolecules , 2000 . 33 ( 5 ): 1848 DOI: 10.1021/ma991427x http://doi.org/10.1021/ma991427x .

C.Z. Zhu , X.F. Liu , X.L. Yu , N. Zhao , J.H. Liu , J. Xu . . Carbon , 2012 . 50 ( 1 ): 235 DOI: 10.1016/j.carbon.2011.08.040 http://doi.org/10.1016/j.carbon.2011.08.040 .

K. Fukuyama , Y. Kasahara , N. Kasahara , A. Oya , K. Nishikawa . . Carbon , 2001 . 39 ( 2 ): 287 DOI: 10.1016/S0008-6223(00)00159-7 http://doi.org/10.1016/S0008-6223(00)00159-7 .

M. Kaburagi , Y.Z. Bin , D. Zhu , C.Y. Xu , M. Matsuo . . Carbon , 2003 . 41 ( 5 ): 915 DOI: 10.1016/S0008-6223(02)00407-4 http://doi.org/10.1016/S0008-6223(02)00407-4 .

C.Z. Zhu , X.L. Yu , X.F. Liu , Y.Z. Mao , R.G. Liu , N. Zhao , X.L. Zhang , J. Xu . . Chinese J. Polym. Sci. , 2013 . 31 ( 5 ): 823 DOI: 10.1007/s10118-013-1272-1 http://doi.org/10.1007/s10118-013-1272-1 .

A. Takaku , M. Shioya . . J. Mater. Sci. , 1986 . 21 ( 12 ): 4443 DOI: 10.1007/BF01106569 http://doi.org/10.1007/BF01106569 .

T.C. Chieu , M.S. Dresselhaus , M. Endo . . Phys. Rev. B , 1982 . 26 ( 10 ): 5867 DOI: 10.1103/PhysRevB.26.5867 http://doi.org/10.1103/PhysRevB.26.5867 .

S.S. Tzeng . . Carbon , 2006 . 44 ( 10 ): 1986 DOI: 10.1016/j.carbon.2006.01.024 http://doi.org/10.1016/j.carbon.2006.01.024 .

F. Tuinstra , J.L. Koenig . . J. Compos. Mater. , 1970 . 4 ( 4 ): 492 .

H.S. Shim , R.H. Hurt , N.Y.C. Yang . . Carbon , 2000 . 38 ( 1 ): 29 DOI: 10.1016/S0008-6223(99)00096-2 http://doi.org/10.1016/S0008-6223(99)00096-2 .

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