Hierarchical Crystalline Structures Induced by Temperature Profile in HDPE Bars during Melt Penetration Process

Chun-xia Zhu; Rui-yan Zhang; Yan-hao Huang; Wei Yang; Zheng-ying Liu; Jian-ming Feng; Ming-bo Yang

doi:10.1007/s10118-017-1880-2

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Hierarchical Crystalline Structures Induced by Temperature Profile in HDPE Bars during Melt Penetration Process

PAPERS | Updated：2021-02-18

- Hierarchical Crystalline Structures Induced by Temperature Profile in HDPE Bars during Melt Penetration Process
- Chinese Journal of Polymer Science Vol. 35, Issue 1, Pages: 108-122(2017)
- Affiliations：
  
  College of Polymer Science and Engineering, State Key Laboratory of Polymer Materials Engineering, Sichuan University, Chengdu 610065, China
- Author bio：
  
  Ming-bo Yang, E-mail:yangmb@scu.edu.cn
- Funds：
- DOI：10.1007/s10118-017-1880-2
  CLC：
- Received：19 May 2016，
  
  Revised：2016-6-23，
  
  Accepted：23 June 2016，
  
  Published：2017-01
- Accepted：
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Chun-xia Zhu, Rui-yan Zhang, Yan-hao Huang, et al. Hierarchical Crystalline Structures Induced by Temperature Profile in HDPE Bars during Melt Penetration Process[J]. Chinese Journal of Polymer Science, 2017, 35(1): 108-122.
DOI：

Chun-xia Zhu, Rui-yan Zhang, Yan-hao Huang, et al. Hierarchical Crystalline Structures Induced by Temperature Profile in HDPE Bars during Melt Penetration Process[J]. Chinese Journal of Polymer Science, 2017, 35(1): 108-122. DOI： 10.1007/s10118-017-1880-2.

摘要

Abstract

The hierarchical crystalline morphologies and orientation structures across the thickness direction in high-density polyethylene (HDPE) molded bars were investigated via a novel melt-penetrating processing method named multi-melt multi-injection molding (M

IM). The samples with various mold temperatures (20

40 and 60℃) were prepared

and the effects of the external temperature profile on the evolution of crystalline microstructures were studied. With scanning electron microscopy (SEM)

the transition of crystalline morphology from ring-banded structure to oriented lamellae was observed with decreasing mold temperature

and the oriented lamellae were formed at the sub-skin layer of the samples at the lowest mold temperature

which was further testified by differential scanning calorimetry (DSC). With the decline of mold temperature

the degree of orientation

obtained from two-dimensional small angle X-ray scattering (2D-SAXS)

was increased and long periods rose a little. Thus

decreasing mold temperature was beneficial to the formation of orientation structures because the relaxation of chains was weakened.

关键词

Keywords

references

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