Solvent Vapor Annealing Induced Polymorphic Transformation of Polybutene-1

Shao Hua-feng; Ma Ya-ping; Nie Hua-rong; He Ai-hua

doi:10.1007/s10118-016-1823-3

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Solvent Vapor Annealing Induced Polymorphic Transformation of Polybutene-1

PAPERS | Updated：2021-05-12

- Solvent Vapor Annealing Induced Polymorphic Transformation of Polybutene-1
- Chinese Journal of Polymer Science Vol. 34, Issue 9, Pages: 1141-1149(2016)
- Affiliations：
  
  Shandong Provincial Key Laboratory of Olefin Catalysis and Polymerization, Key Laboratory of Rubber-Plastics(Ministry of Education), School of Polymer Science and Engineering, Qingdao University of Science and Technology, Qingdao 266042, China
- Author bio：
  
  Hua-rong Nie(聂华荣),E-mail:niehr@iccas.ac.cn
  Ai-hua He(贺爱华),E-mail:aihuahe@iccas.ac.cn,ahhe@qust.edu.cn
- Funds：
- DOI：10.1007/s10118-016-1823-3
  CLC：
- Received：17 March 2016，
  
  Revised：2016-4-20，
  
  Accepted：20 April 2016，
  
  Published：05 October 2016
- Accepted：
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Shao Hua-feng, Ma Ya-ping, Nie Hua-rong, et al. Solvent Vapor Annealing Induced Polymorphic Transformation of Polybutene-1[J]. Chinese Journal of Polymer Science, 2016, 34(9): 1141-1149.
DOI：

Shao Hua-feng, Ma Ya-ping, Nie Hua-rong, et al. Solvent Vapor Annealing Induced Polymorphic Transformation of Polybutene-1[J]. Chinese Journal of Polymer Science, 2016, 34(9): 1141-1149. DOI： 10.1007/s10118-016-1823-3.

摘要

Abstract

Solvent annealing is a facile method for changing the aggregated microstructure and physical properties of polymer materials. In this paper

we addressed the effects of solvent vapor annealing

including chloroform and water vapor

on the polymorphic transformation in both hot-pressed film and electrospun nonwoven of isotactic polybutene-1 (PB-1) by means of

in situ

Fourier transform infrared spectroscopy (FTIR). The pretty rapid transition rate caused by the increased motion of molecular chains under chloroform vapor is associated with a lowest crystallinity. Also

a decreased crystallinity with the crystal transition occurred in electrospun nonwovens resulting from the relaxation of the stretched molecular chains into amorphous state rather than realignment into crystal form I predominating the crystal transition process.

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Keywords

references

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