Facile Fabrication of High-performance Polyimide Nanocomposites with <italic style="font-style: italic">in situ</italic> Formed “Impurity-free” Dispersants

Jing-jing Shen; Dong-ge Zhang; Xing Liu; Yu-chang Tang; Yu Lin; Guo-zhang Wu

doi:10.1007/s10118-016-1771-y

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Facile Fabrication of High-performance Polyimide Nanocomposites with in situ Formed “Impurity-free” Dispersants

PAPERS | Updated：2021-05-12

- Facile Fabrication of High-performance Polyimide Nanocomposites with in situ Formed “Impurity-free” Dispersants
- Chinese Journal of Polymer Science Vol. 34, Issue 5, Pages: 532-541(2016)
- Affiliations：
  
  Shanghai Key Laboratory of Advanced Polymeric Materials, School of Materials Science and Engineering, East China University of Science and Technology, Shanghai 200237, China
- Author bio：
  
  Yu Lin (林宇), E-mail: linyu@ecust.edu.cn
  Guo-zhang Wu (吴国章), E-mail: wgz@ecust.edu.cn
- Funds：
- DOI：10.1007/s10118-016-1771-y
  CLC：
- Received：28 October 2015，
  
  Revised：2015-12-19，
  
  Accepted：22 December 2015，
  
  Published：2016-05
- Accepted：
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Jing-jing Shen, Dong-ge Zhang, Xing Liu, et al. Facile Fabrication of High-performance Polyimide Nanocomposites with in situ Formed “Impurity-free” Dispersants[J]. Chinese Journal of Polymer Science, 2016, 34(5): 532-541. DOI: 10.1007/s10118-016-1771-y.
DOI：

Jing-jing Shen, Dong-ge Zhang, Xing Liu, et al. Facile Fabrication of High-performance Polyimide Nanocomposites with in situ Formed “Impurity-free” Dispersants[J]. Chinese Journal of Polymer Science, 2016, 34(5): 532-541. DOI: 10.1007/s10118-016-1771-y. DOI：

摘要

Abstract

Polyimide/carbon black (PI/CB) nanocomposite films were fabricated

via

the direct ball-milling method with poly(amic acid) (PAA)

the precursor of PI

as an

in situ

formed impurity-free dispersant. FTIR and Raman spectral results reveal that

besides physical adsorption

chemical grafting of PAA chains onto the CB surface occurs during the ball-milling process. Comparative studies show that introduction of various commercial dispersants improves the dispersion of CB. However

the mixtures exhibit poor reproducibility

unstable electrical properties

and decreased tensile strength; these issues may be attributed to interfacial pollution brought about by differences in the chemical structures of the dispersant and the matrix. The impurity-free dispersant is effective not only in ensuring the uniform dispersion of CB particles but also in enhancing filler-matrix interfacial adhesion. High-molecular weight PAA chains are effective reagents for impurity-free modification and can therefore be used to improve the electrical and mechanical properties of the resultant composite.

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Facile Fabrication of High-performance Polyimide Nanocomposites with in situ Formed “Impurity-free” Dispersants

DOI：10.1007/s10118-016-1771-y

摘要

Abstract

关键词

Keywords

references