SYNTHESIS AND CHARACTERIZATION OF FUNCTIONALIZED CARBON BLACK/POLY(VINYL ALCOHOL) HIGH REFRACTIVE INDEX NANOCOMPOSITES

Peng-fei Xue; Ji-bin Wang; Yu-bin Bao; Qiu-ying Li; Chi-fei Wu

doi:10.1007/s10118-012-1152-0

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SYNTHESIS AND CHARACTERIZATION OF FUNCTIONALIZED CARBON BLACK/POLY(VINYL ALCOHOL) HIGH REFRACTIVE INDEX NANOCOMPOSITES

PAPER | Updated：2023-01-03

- SYNTHESIS AND CHARACTERIZATION OF FUNCTIONALIZED CARBON BLACK/POLY(VINYL ALCOHOL) HIGH REFRACTIVE INDEX NANOCOMPOSITES
- Chinese Journal of Polymer Science Vol. 30, Issue 5, Pages: 652-663(2012)
- Affiliations：
  
  a.Polymer Alloy Laboratory and Key Laboratory of Ultrafine Materials of Ministry of Education, East China University of Science and Technology, Shanghai 200237, China
  b.Shanghai Key Laboratory Polymeric Materials, East China University of Science and Technology, Shanghai 200237, China
- Author bio：
  
  **Qiu-ying Li (李秋影), E-mail: liqy@ecust.edu.cn
- Funds：
- DOI：10.1007/s10118-012-1152-0
  CLC：
- Received：24 October 2011，
  
  Revised：2011-12-07，
  
  Accepted：15 December 2011，
  
  Published：2012-09
- Accepted：
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Peng-fei Xue, Ji-bin Wang, Yu-bin Bao, et al. SYNTHESIS AND CHARACTERIZATION OF FUNCTIONALIZED CARBON BLACK/POLY(VINYL ALCOHOL) HIGH REFRACTIVE INDEX NANOCOMPOSITES[J]. Chinese Journal of Polymer Science, 2012, 30(5): 652-663.
DOI：

Peng-fei Xue, Ji-bin Wang, Yu-bin Bao, et al. SYNTHESIS AND CHARACTERIZATION OF FUNCTIONALIZED CARBON BLACK/POLY(VINYL ALCOHOL) HIGH REFRACTIVE INDEX NANOCOMPOSITES[J]. Chinese Journal of Polymer Science, 2012, 30(5): 652-663. DOI： 10.1007/s10118-012-1152-0.

摘要

Abstract

Carbon black (CB)/polymer composites with high refractive index (RI) were fabricated from poly(vinyl alcohol) (PVA) and covalently functionalized nano-CB (PVA-es-CB) by simple esterification reaction. Transmission electron microscopy showed that uniform aggregates of PVA-es-CB nanoparticles with a size smaller than 100 nm formed in the nanocomposite films. Ellipsometric measurements indicated that the PVA-es-CB/PVA composite films had a RI in the range 1.520-1.598 linearly increased with the PVA-es-CB volume content. Theoretical equation based on Lorentz-Lorenz theory provided reasonably close estimation of the refractive indices to the experimentally observed values. The hybrid films also revealed relatively good surface planarity

thermal stability and optical transparency.

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