SYNTHESIS AND CHARACTERIZATION OF SCHIFF-BASE-CONTAINING POLYAMIDES

Mousa Ghaemy; Hossein Mighani; Raouf Alizadeh

doi:10.1007/s10118-010-1004-8

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SYNTHESIS AND CHARACTERIZATION OF SCHIFF-BASE-CONTAINING POLYAMIDES

Paper | Updated：2021-06-21

- SYNTHESIS AND CHARACTERIZATION OF SCHIFF-BASE-CONTAINING POLYAMIDES
- Chinese Journal of Polymer Science Vol. 29, Issue 2, Pages: 149-155(2011)
- Affiliations：
  
  Department of Chemistry, Mazandaran University, Babolsar, Iran
- Author bio：
  
  *Mousa Ghaemy, E-mail: ghaemy@umz.ac.ir
- Funds：
- DOI：10.1007/s10118-010-1004-8
  CLC：
- Received：14 January 2010，
  
  Revised：2010-03-08，
  
  Accepted：19 March 2010，
  
  Published：2011
- Accepted：
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Mousa Ghaemy, Hossein Mighani, Raouf Alizadeh. SYNTHESIS AND CHARACTERIZATION OF SCHIFF-BASE-CONTAINING POLYAMIDES[J]. Chinese Journal of Polymer Science, 2011, 29(2): 149-155.
DOI：

Mousa Ghaemy, Hossein Mighani, Raouf Alizadeh. SYNTHESIS AND CHARACTERIZATION OF SCHIFF-BASE-CONTAINING POLYAMIDES[J]. Chinese Journal of Polymer Science, 2011, 29(2): 149-155. DOI： 10.1007/s10118-010-1004-8.

摘要

Abstract

A series of new Schiff base polyamides (PAs) were synthesized by polycondensation of benzilbisthiosemicarbazone diamine (LH

) with different commercially available aliphatic and aromatic diacid chlorides. The monomer and all the PAs were characterized by FTIR

H-NMR

and elemental analysis. The prepared polyamides showed inherent viscosities in the range of 0.30-0.36 dL/g in DMF at 25℃

indicating their moderate molecular weight. The PAs were completely soluble in aprotic polar solvents such as dimethylformamide (DMF)

-methylpyrolidone (NMP)

tetrachloroethane (TCE)

dimthylsulfoxide (DMSO) and also in H

and partially soluble in THF

acetone and chloroform at room temperature. Thermal analysis showed that these PAs were practically amorphous and exhibited 10% weight loss above 220℃.

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