NANOMECHANICAL MAPPING OF CARBON BLACK REINFORCED NATURAL RUBBER BY ATOMIC FORCE MICROSCOPY
Feature Article|Updated:2021-06-21
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NANOMECHANICAL MAPPING OF CARBON BLACK REINFORCED NATURAL RUBBER BY ATOMIC FORCE MICROSCOPY
Issue 1, Pages: 35-41(2007)
Affiliations:
1. Department of Organic and Polymeric Materials Graduate School of Science and Engineering
2. Tokyo Institute of Technology
3. 2-12-1 O-okayama
4. Meguro-ku
5. Tokyo ,152-8552
6. Japan
Author bio:
Funds:
DOI:
CLC:TQ330.1
Published:2007
Accepted:
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[1]Toshio Nishi,Hideyuki Nukaga,So Fujinami,Ken Nakajima.NANOMECHANICAL MAPPING OF CARBON BLACK REINFORCED NATURAL RUBBER BY ATOMIC FORCE MICROSCOPY[J].Chinese Journal of Polymer Science,2007(01):35-41.
NANOMECHANICAL MAPPING OF CARBON BLACK REINFORCED NATURAL RUBBER BY ATOMIC FORCE MICROSCOPY[J]. 2007, (1): 35-41.
[1]Toshio Nishi,Hideyuki Nukaga,So Fujinami,Ken Nakajima.NANOMECHANICAL MAPPING OF CARBON BLACK REINFORCED NATURAL RUBBER BY ATOMIC FORCE MICROSCOPY[J].Chinese Journal of Polymer Science,2007(01):35-41.DOI:
NANOMECHANICAL MAPPING OF CARBON BLACK REINFORCED NATURAL RUBBER BY ATOMIC FORCE MICROSCOPY[J]. 2007, (1): 35-41.DOI:
NANOMECHANICAL MAPPING OF CARBON BLACK REINFORCED NATURAL RUBBER BY ATOMIC FORCE MICROSCOPY
<正>Atomic force microscopy (AFM) has the advantage of obtaining mechanical properties as well as topographic information at the same time. By analyzing force-distance curves measured over two-dimensional area using Hertzian contact mechanics
Young’s modulus mapping was obtained with nanometer-scale resolution. Furthermore
the sample deformation by the force exerted was also estimated from the force-distance curve analyses. We could thus reconstruct a real topographic image by incorporating apparent topographic image with deformation image. We applied this method to carbon black reinforced natural rubber to obtain Young’s modulus distribution image together with reconstructed real topographic image. Then we were able to recognize three regions; rubber matrix
carbon black (or bound rubber) and intermediate regions. Though the existence of these regions had been investigated by pulsed nuclear magnetic resonance
this paper would be the first to report on the quantitative evaluation of the interfacial region in real space.
Abstract
Atomic force microscopy (AFM) has the advantage of obtaining mechanical properties as well as topographic information at the same time. By analyzing force-distance curves measured over two-dimensional area using Hertzian contact mechanics
Young’s modulus mapping was obtained with nanometer-scale resolution. Furthermore
the sample deformation by the force exerted was also estimated from the force-distance curve analyses. We could thus reconstruct a real topographic image by incorporating apparent topographic image with deformation image. We applied this method to carbon black reinforced natural rubber to obtain Young’s modulus distribution image together with reconstructed real topographic image. Then we were able to recognize three regions; rubber matrix
carbon black (or bound rubber) and intermediate regions. Though the existence of these regions had been investigated by pulsed nuclear magnetic resonance
this paper would be the first to report on the quantitative evaluation of the interfacial region in real space.
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