MICRO-PHASE SEPARATION IN EPOXY RESIN WATERBORNE PARTICLES DURING CURING PROCESS

Xi-yan Liu; Dong Qiu; Mei-li Guo; Zhen-zhong Yang

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MICRO-PHASE SEPARATION IN EPOXY RESIN WATERBORNE PARTICLES DURING CURING PROCESS

Note | Updated：2021-06-21

- MICRO-PHASE SEPARATION IN EPOXY RESIN WATERBORNE PARTICLES DURING CURING PROCESS
- Vol. 23, Issue 5, Pages: 561-566(2005)
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- Published：20 September 2005
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Xi-yan Liu, Dong Qiu, Mei-li Guo, et al. MICRO-PHASE SEPARATION IN EPOXY RESIN WATERBORNE PARTICLES DURING CURING PROCESS[J]. 2005, 23(5): 561-566.
DOI：

Xi-yan Liu, Dong Qiu, Mei-li Guo, et al. MICRO-PHASE SEPARATION IN EPOXY RESIN WATERBORNE PARTICLES DURING CURING PROCESS[J]. 2005, 23(5): 561-566. DOI：

摘要

Sub-micron sized phenolic epoxy resin waterborne particles were prepared by phase inversion emulsification. Micro-phase separation occurred during the curing process at high temperature. The as-prepared samples possessed one glass transition temperature (Tg) and two exothermal processes during DSC heating scannings. After being thermally treated above the exothermal peak temperature

they possessed two glass transition temperatures with the disappearance of exothermal peaks

whilst a core/shell structure was formed. This was likely related with the outward diffusion of reactive oligomers to the outer layer of particles.

Abstract

they possessed two glass transition temperatures with the disappearance of exothermal peaks

whilst a core/shell structure was formed. This was likely related with the outward diffusion of reactive oligomers to the outer layer of particles.

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