PREPARATION OF NANOMETER TiO2 ORGANIC SOLUTION —EFFECT OF ORGANIC SILOXANE ON SOL PROPERTIES*

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PREPARATION OF NANOMETER TiO2 ORGANIC SOLUTION —EFFECT OF ORGANIC SILOXANE ON SOL PROPERTIES*

Papers | Updated：2021-06-21

- PREPARATION OF NANOMETER TiO2 ORGANIC SOLUTION —EFFECT OF ORGANIC SILOXANE ON SOL PROPERTIES*
- Vol. 22, Issue 3, Pages: 247-251(2004)
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- Published：20 June 2004
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PREPARATION OF NANOMETER TiO2 ORGANIC SOLUTION —EFFECT OF ORGANIC SILOXANE ON SOL PROPERTIES*[J]. 2004, 22(3): 247-251.
DOI：

PREPARATION OF NANOMETER TiO2 ORGANIC SOLUTION —EFFECT OF ORGANIC SILOXANE ON SOL PROPERTIES*[J]. 2004, 22(3): 247-251. DOI：

摘要

A homogeneous longtime stabilized transparent nanometer TiO2 organic solution was obtained by means of the simultaneous hydrolysis and co-polycodensation of tetrabutyltitanate (TBT) and methacryloxypropyltrimethoxysilane (MAPTMS) by the sol-gel process. The particle size of nanometer titanium dioxide was controlled by use of bifunctional silanes

such as diphenyldimethoxysilane (DPDMS)

diphenyldiethoxysilane (DPDES) and dimethyldiethoxysilane (DMDES). The effect of TiO2 content in the solution on the refractive index of system was discussed in detail. The result shows that the refractive index of solution increases linearly with TiO2 content. The refractive index of the three hybrid nanometer materials attained 1.6053

1.5846 and 1.5346

respectively. The size of nanometer particles was characterized by TEM and the particle diameter thus obtained is in the range of 20-90 nm. FT-IR spectra of the materials show that the Ti— O—Si bond is formed.

Abstract

such as diphenyldimethoxysilane (DPDMS)

1.5846 and 1.5346

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