SYNTHESIS OF ORGANOMETALLIC PRECURSORS FOR Si/Zr/C/N-BASED CERAMICS*

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SYNTHESIS OF ORGANOMETALLIC PRECURSORS FOR Si/Zr/C/N-BASED CERAMICS*

Papers | Updated：2021-06-21

- SYNTHESIS OF ORGANOMETALLIC PRECURSORS FOR Si/Zr/C/N-BASED CERAMICS*
- Vol. 21, Issue 1, Pages: 99-101(2003)
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- Published：20 February 2003
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SYNTHESIS OF ORGANOMETALLIC PRECURSORS FOR Si/Zr/C/N-BASED CERAMICS*[J]. 2003, 21(1): 99-101.
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SYNTHESIS OF ORGANOMETALLIC PRECURSORS FOR Si/Zr/C/N-BASED CERAMICS*[J]. 2003, 21(1): 99-101. DOI：

摘要

A new kind of organometallic precursor for Si/Zr/C/N-based ceramics was synthesized from the amine exchangereaction of hexamethylcyclotrisilazane (D3N) and tetrakis(diethylamino) zirconium (Zr[NEt2]4). Pyrolysis was performedunder nitrogen at 800℃ in a tube furnace equipped with a temperature program controller. The highest pyrolytic yield was67.5%.

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