IN-SITU AFM OF POLYMER CRYSTALLIZATION

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IN-SITU AFM OF POLYMER CRYSTALLIZATION

Papers | Updated：2021-06-21

- IN-SITU AFM OF POLYMER CRYSTALLIZATION
- Vol. 21, Issue 2, Pages: 135-140(2003)
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- Published：20 April 2003
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IN-SITU AFM OF POLYMER CRYSTALLIZATION[J]. 2003, 21(2): 135-140.
DOI：

IN-SITU AFM OF POLYMER CRYSTALLIZATION[J]. 2003, 21(2): 135-140. DOI：

摘要

Atomic force microscopy images taken during the crystallization of polyethylene both from processed andquiescent melts are presented. Crystallization from processed melts provides further evidence of a region in front of agrowing lamella that is influenced by the crystallization process

but extending only 40 nm into the melt. High-resolutionimages of the growing crystal tip

taken during crystallization

show no direct evidence of the existence of intermediatephases. The growing tip is shown to be slightly rounded.In-filling crystallization

occurring after the initial flush of growth

is imaged in polyethylene for the first time

and shown to continue to a temperature 8℃ below the initial crystallization temperature.

Abstract

but extending only 40 nm into the melt. High-resolutionimages of the growing crystal tip

taken during crystallization

show no direct evidence of the existence of intermediatephases. The growing tip is shown to be slightly rounded.In-filling crystallization

occurring after the initial flush of growth

is imaged in polyethylene for the first time

and shown to continue to a temperature 8℃ below the initial crystallization temperature.

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