THE HYDROSILYLATION REACTION OF LADDERLIKE POLYVINYLSILSESQUIOXANE WITH 1, 1, 3, 3-TETRAMETHYLDISILOXANE*

CAO Xinyu; XU Hui; WANG Letian; LI Ze; CAO Ming; XIE Ping; ZHANG Rongben; ZHU Chuanfeng; WANG Chen

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THE HYDROSILYLATION REACTION OF LADDERLIKE POLYVINYLSILSESQUIOXANE WITH 1, 1, 3, 3-TETRAMETHYLDISILOXANE*

Papers | Updated：2021-06-21

- THE HYDROSILYLATION REACTION OF LADDERLIKE POLYVINYLSILSESQUIOXANE WITH 1, 1, 3, 3-TETRAMETHYLDISILOXANE*
- Vol. 16, Issue 3, Pages: 226-233(1998)
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- Published：20 September 1998
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CAO Xinyu, XU Hui, WANG Letian, et al. THE HYDROSILYLATION REACTION OF LADDERLIKE POLYVINYLSILSESQUIOXANE WITH 1, 1, 3, 3-TETRAMETHYLDISILOXANE*[J]. 1998, 16(3): 226-233.
DOI：

CAO Xinyu, XU Hui, WANG Letian, et al. THE HYDROSILYLATION REACTION OF LADDERLIKE POLYVINYLSILSESQUIOXANE WITH 1, 1, 3, 3-TETRAMETHYLDISILOXANE*[J]. 1998, 16(3): 226-233. DOI：

摘要

The hydrosilylation reaction of ladderlike polyvinylsilsesquioxane (Vi-T)with 1

3-tetramethyldisiloxane (H- MM ) catalyzed by dicyclopentadienyl-dichloroplat-inium (Cp2PtCl2) was carried out well in tetrahydrofuran (THF) to produce a soluble whitesolid. This product was characterized by IR

1H-NMR

13C-NMR

29Si-NMR

DSC

X-raydiffraction method

gel permeation chromatography (GPC)

vapour pressure osmometry(VPO)

atomic force microscopy (AFM) and molecular simulation. These results prove that the product contains nanoscale tubular structure.

Abstract

The hydrosilylation reaction of ladderlike polyvinylsilsesquioxane (Vi-T)with 1

1H-NMR

13C-NMR

29Si-NMR

DSC

X-raydiffraction method

gel permeation chromatography (GPC)

vapour pressure osmometry(VPO)

atomic force microscopy (AFM) and molecular simulation. These results prove that the product contains nanoscale tubular structure.

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