Investigating the Absorption and Desorption Behavior of Methylene Chloride in the Poly(aryl ether ketone) Film with Different Crystallinities

Hong-Ru Yang; Jin-Dong Zhang; Dong-Ting Gao; Gang Liu; Chun-Hai Chen; Jia-Nan Yao

doi:10.1007/s10118-023-3046-8

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Investigating the Absorption and Desorption Behavior of Methylene Chloride in the Poly(aryl ether ketone) Film with Different Crystallinities

RESEARCH ARTICLE | Updated：2024-01-12

- Investigating the Absorption and Desorption Behavior of Methylene Chloride in the Poly(aryl ether ketone) Film with Different Crystallinities
- Chinese Journal of Polymer Science Vol. 42, Issue 2, Pages: 239-246(2024)
- Affiliations：
  
  Center for Advanced Low-Dimension Materials, State Key Laboratory for Modification of Chemical Fibers and Polymer Materials, College of Materials Science and Engineering, Donghua University, Shanghai 201620, China
- Author bio：
  
  yjn@dhu.edu.cn
- Funds：
- DOI：10.1007/s10118-023-3046-8
  CLC：
- Received：19 June 2023，
  
  Revised：2023-8-16，
  
  Accepted：21 August 2023，
  
  Online First：19 September 2023，
  
  Published：01 February 2024
- Accepted：
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Yang, H. R.; Zhang, J. D.; Gao, D. T.; Liu, G.; Chen, C. H.; Yao, J. N. Investigating the absorption and desorption behavior of methylene chloride in the poly(aryl ether ketone) film with different crystallinities. Chinese J. Polym. Sci. 2024, 42, 239–246

Hong-Ru Yang, Jin-Dong Zhang, Dong-Ting Gao, et al. Investigating the Absorption and Desorption Behavior of Methylene Chloride in the Poly(aryl ether ketone) Film with Different Crystallinities[J]. Chinese Journal of Polymer Science, 2024, 42(2): 239-246.
Yang, H. R.; Zhang, J. D.; Gao, D. T.; Liu, G.; Chen, C. H.; Yao, J. N. Investigating the absorption and desorption behavior of methylene chloride in the poly(aryl ether ketone) film with different crystallinities. Chinese J. Polym. Sci. 2024, 42, 239–246 DOI： 10.1007/s10118-023-3046-8.

Hong-Ru Yang, Jin-Dong Zhang, Dong-Ting Gao, et al. Investigating the Absorption and Desorption Behavior of Methylene Chloride in the Poly(aryl ether ketone) Film with Different Crystallinities[J]. Chinese Journal of Polymer Science, 2024, 42(2): 239-246. DOI： 10.1007/s10118-023-3046-8.

摘要

The attenuated total reflection Fourier transform infrared spectroscopy analyses was employed to investigate the diffusion behavior of CH

in PAEK films with different crystallinities. According to the Fickian diffusion model

the diffusion coefficients of CH

in PAEK films were calculated.

Abstract

Poly(aryl ether ketone) (PAEK) films with different crystallinities were obtained by controlling the cooling rate

which were subjected to the absorption and desorption of methylene chloride (CH

). We employed attenuated total reflection Fourier transform infrared (ATR-FTIR) spectroscopy analyses to investigate the diffusion behavior of CH

in PAEK films with different crystallinities. According to the Fickian diffusion model

the calculated diffusion coefficients of CH

in PAEK films were observed to decrease with increasing crystallinity. The effect of CH

absorption and desorption on the mechanical properties of PAEK films with different crystallinity was further analyzed using tensile tests. The tensile tests exhibited that CH

has two concurrent effects: plasticization and solvent-induced crystallization. Differential scanning calorimetry (DSC) and wide-angle X-ray diffraction (WXRD) techniques further confirmed solvent-induced crystallization behavior. The results would be beneficial to understand the solvent resistance of PAEK materials and consequently provide the practical application conditions of PAEK with a theoretical basis.

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